北京純水TOC分析儀介紹 水樣中TOC的分析步驟
水中的有機(jī)物質(zhì)的含量,以有機(jī)物中的主要元素一碳的量來表示,稱為總有機(jī)碳。TOC的測定類似于TOD的測定。在950℃的高溫下,使水樣中的有機(jī)物氣化燃燒,生成CO2,通過紅外線分析儀,測定其生成的CO2之量,即可知總有機(jī)碳量。
北京純水TOC分析儀介紹 水中TOC的監(jiān)測
我們的生活離不開水,若相當(dāng)多的有機(jī)污染物存在于水中,將直接影響水體的質(zhì)量,對我們的生活和生產(chǎn)造成危害,因此水和廢水的監(jiān)測,越來越引起人們的重視。其中水體中總有機(jī)碳(TOC)含量的檢測,日益引起關(guān)注。它是以碳含量表示水體中有機(jī)物質(zhì)總量的綜合指標(biāo)。TOC的測定一般采用燃燒法,此法能將水樣中有機(jī)物全部氧化,可以很直接地用來表示有機(jī)物的總量。因而它被作為評價(jià)水體中有機(jī)物污染程度的一項(xiàng)重要參考指標(biāo)。
Analysis steps of TOC in water samples
The content of organic matter in water, expressed by the amount of carbon, the main element in organic matter, is called total organic carbon. The determination of TOC is similar to the determination of TOD. At a high temperature of 950℃, the organic matter in the water sample is gasified and burned to generate CO2. The total organic carbon content can be determined by measuring the amount of CO2 generated through an infrared analyzer.
Monitoring of TOC in water
Our lives cannot do without water. If a considerable amount of organic pollutants exist in water, it will directly affect the quality of the water and cause harm to our lives and production. Therefore, the monitoring of water and wastewater is increasingly attracting people's attention. The detection of total organic carbon (TOC) content in water bodies is increasingly attracting attention. It is a comprehensive indicator that represents the total amount of organic matter in water using carbon content. The determination of TOC generally adopts the combustion method, which can oxidize all organic matter in the water sample and can be directly used to represent the total amount of organic matter. Therefore, it is regarded as an important reference indicator for evaluating the degree of organic matter pollution in water bodies.
主要技術(shù)參數(shù)
電 源:220V?22V
電源頻率:50Hz?1Hz
額定功率:100W
基本尺寸:44cm?18cm?26cm
檢測極限:0.001mg/L
檢測精度:?5%
檢測范圍:0.001mg/L~1.000mg/L
分析時(shí)間:4min
響應(yīng)時(shí)間:15 min以內(nèi)
樣品溫度:1-95℃
環(huán)境溫度:10-40℃ 溫度變化在?5℃/d以內(nèi)
Main technical parameters
Power supply: 220V?22V
Power frequency: 50Hz?1Hz
Rated power: 100W
Basic size: 44cm?18cm?26cm
Detection limit: 0.001mg/L
Detection accuracy:?5%
Detection range: 0.001mg/L~1.000mg/L
Analysis time: 4 minutes
Response time: within 15 minutes
Sample temperature: 1-95℃
Environmental temperature: 10-40℃Temperature variation within?5℃/d
運(yùn)行要求
1交流電源:170~260 V,頻率:50/60 Hz;
2分析儀的量程是:電導(dǎo)率< 10.0 us/cm;TOC < 1.0 PPM。如果水樣中的無
機(jī)碳或有機(jī)碳濃度超出了儀器的檢測范圍,需使用高純水或有機(jī)碳濃度較
低的去離子水沖洗管路。
3儀器運(yùn)行的環(huán)境溫度5℃ –40℃。
安全措施忠告:
1.請保證電源可靠接地;
2.電源電纜線的線徑> 2.5 mm2;
3.請勿將儀器浸泡于水或其它液體中。
Operational requirements
1. AC power supply: 170-260 V, frequency: 50/60 Hz;
The range of the 2 analyzer is: conductivity<10.0 us/cm; TOC<1.0 PPM. If there is no
The concentration of organic carbon or organic carbon exceeds the detection range of the instrument, and it is necessary to use high-purity water or organic carbon with a lower concentration
Flush the pipeline with low deionized water.
The ambient temperature for instrument operation is 5℃-40℃.
Safety measures and advice:
1. Please ensure that the power supply is reliably grounded;
2. The wire diameter of the power cable is>2.5 mm2;
3. Do not immerse the instrument in water or other liquids.
使用與操作方法
開始檢測并計(jì)入檢測次數(shù),檢測完畢后顯示最后一次檢測結(jié)果,其中幾次檢測的結(jié)果均自動(dòng)保存在查詢記錄當(dāng)中。檢測次數(shù)的設(shè)置方式為:用“選擇”鍵移動(dòng)光標(biāo),用“設(shè)置”鍵修改數(shù)字,按“確定”鍵進(jìn)行確認(rèn),進(jìn)入分析界面。先進(jìn)行四次沖洗過程
Usage and operation methods
Start testing and count the number of tests. After testing, the last test result will be displayed, and the results of several tests will be automatically saved in the query record. The setting method for the number of detections is: use the "Select" key to move the cursor, use the "Set" key to modify the number, press the "OK" key to confirm, and enter the analysis interface. Perform four flushing processes first
試劑準(zhǔn)備
(1)鄰苯二甲酸氫鉀(KHC8H4O4):基準(zhǔn)試劑
(2)無水碳酸鈉:基準(zhǔn)試劑
(3)碳酸氫鈉:基準(zhǔn)試劑
(4)無二氧化碳蒸餾水
Reagent preparation
(1) Potassium hydrogen phthalate (KHC8H4O4): reference reagent
(2) Anhydrous sodium carbonate: reference reagent
(3) Sodium bicarbonate: reference reagent
(4) Carbon dioxide free distilled water
故障現(xiàn)象:
顯示屏出現(xiàn)“UV燈已過期”/“泵管已過期” ;
故障原因:
1) 耗材使用已過期;
2) 更換耗材后沒有清空耗材運(yùn)行記錄;
解決方法:
1) 更換耗材;
2) 更換耗材后,清空耗材運(yùn)行時(shí)間;
Fault symptom:
The display screen shows "UV light has expired"/"pump tube has expired";
Fault cause:
1) The use of consumables has expired;
2) Failure to clear the operating records of consumables after replacing them;
Solution:
1) Replace consumables;
2) After replacing consumables, clear the running time of consumables;
應(yīng)用范圍
該儀器可用于檢測制藥工業(yè)中純化水、注射用水和去離子水中有機(jī)碳的濃度;也可用于半導(dǎo)體行業(yè)中超純水TOC的檢測。
在制藥領(lǐng)域和生物化學(xué)領(lǐng)域清潔驗(yàn)證過程中,可用于驗(yàn)證清潔效果。
該儀器具有在線檢測功能,可以在線監(jiān)測制藥工業(yè)的制水系統(tǒng)、半導(dǎo)體工業(yè)的超純水制備系統(tǒng)和晶片工藝過程、電廠去離子水制備過程等。
Application scope
This instrument can be used to detect the concentration of organic carbon in purified water, injection water, and deionized water in the pharmaceutical industry; It can also be used for the detection of ultra-pure water TOC in the semiconductor industry.
In the cleaning validation process in the pharmaceutical and biochemical fields, it can be used to verify the cleaning effect.
This instrument has online detection function, which can monitor the water preparation system in the pharmaceutical industry, the ultra pure water preparation system and wafer process in the semiconductor industry, and the deionized water preparation process in power plants.
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